ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Streicher Test). ASTM A practice – Free download as Excel Spreadsheet .xls /.xlsx), PDF File .pdf), Text File .txt) or read online for free. ASTM A Practice B test. In this test a sample of surface area cm. 2 is exposed for a period of hours to boiling solution of 50% H2SO4 + %.
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In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. Rockwell or Superficial Hardness.
This method is a hour boiling test for “as received” specimens of stainless steel. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.
ASTM A Intergranular Corrosion Testing and Analysis
There is several cause for SCC, Chloride is the leading cause of transgranular cracking or attack. Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. This specification is for detecting susceptibility to intergranular attack IGA.
Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required. These practices include five intergranular corrosion tests, namely: Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.
Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. The first and fastest step is the ASTM A Practice A, a ast, same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion.
Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. In everyday applications, corrosion varies by materials and solutions.
It depends on which Practice is selected, but typically ranges from aastm days for different tests.
Intergranular Corrosion Testing: An Overview of ASTM A262
Historical Version s – view previous versions of standard Work Prcatice s – proposed revisions of this standard Translated Version s: For example, many low-carbon and stabilized stainless steels e. A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. The chart below comes lractice the ASTM A standard for selection of the appropriate test by alloy type:.
A recent publication on intergranular corrosion. Similar to the G test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades. This method is preferable for chromium depletions and corrosion in intermetallic phases.
A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens.
The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either sstm or “Suspect”. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
Historical Version s – view aztm versions of standard. Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. See Appendix X1 for information regarding test selection.
The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. All austenitic stainless steels should meet this requirement, if proper annealing took place. Discover perspectives, resources, and advice from our world-leading Engaged Experts. Please share this page: This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means.
Link to Active This link will always route to the current Active version of the standard. Work Item s – proposed revisions of this standard. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.
If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed. If the structure is acceptable no additional testing is required. The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use.
Because it can be run quickly for screening, we often run this test first. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur. If you are not sure, please contact us for assistance. Intergranular corrosion shows up as the dark black lines around the grain boundaries.
This abstract is a brief summary of the referenced standard. For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while n of carbides may occur somewhat less oxidizing solutions.
Contact us now for pricing or a quote! ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility.
Vickers Hardness 5Kg and 10Kg. Like what you saw? All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.